美国标准 ASTM D 6400 环保降解材料测试
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Test item 测试名称: Biodegradability 环保降解材料
Norm Refer 涉及标准:DIN V 54900, EN 13432, ASTM D 5388, ISO 16929,OECD 208, ASTM D 6868, NF T51-800
Test info 测试内容:
化学测试,Chemical Characteristic Test
生物降解能力测试,Biodegradability test
生物分解, Disintegration test
生态无毒测试, Ecotoxicity test: Plant
这些测试可以保证没有重金属进入土壤并没有副作用
Brief Summary of ASTM D 6400 & ASTM D 6868
Both ASTM D6400 and ASTM D6868 include the same three components of testing (the difference between the specification is that the criteria themselves are slightly different).
1.Disintegration During Composting (on final product) • Measured the by physical breakdown of product to pass a 2mm sieve
2.Inherent Biodegradation(on individual constituents)
• Measured by carbon dioxide (CO2)evolution as the product biodegrades
• Or some materials can qualify for the “materials of natural original”exception in which case biobased content must be measured by ASTM D6866
3.No Adverse Impacts on the Ability of Compost to Support Plant Growth (on final product)
• Testing for heavy metals
• Plant Growth Study
In addition, the material must be chemically characterized to defend product claims:
FTIR & Ash Content (to help with fingerprinting the material)
Density (grammage) for bagasse and paper based products.
Which Standard Applies to Your Product?
ASTM D 6400 塑料is to be used for plastic products
ASTM D 6868 纸制品is used for products such as molded pulp products or coated paper, basically non-plastic items (may be an oversimplification, but expresses the general idea).
Sample size 送样规格:5000g
Lead time 测试周期: 常规 Regular 5-8 months working days
FTIR, ash content, and regulated metals plus flourine – 3 weeks (can be done quicker if needed)
Biobased testing (ASTM D6866) – approximately 7 work days
Disintegration – about 18 weeks; includes 12 weeks of composting plus a bit of time to set up the test, then at the end of the test to make the final measurements and type the report
Ecotoxicity – about 3-4 weeks, this starts at the end of disintegration testing though
Biodegradation – up to 180 days (plus 2 weeks for setup & reporting) or as few as 45 days (plus 2 weeks); it is dependent on how fast the material biodegrades, not on how fast we work.
Reference Picture 参考图片:
Others 其他信息:
1、体外试验是将样品浸泡在溶液中,不同时间点,取出样品称重,根据重量变化看材料有无降解,
2、体内试验是将样品植入到动物皮下组织,不同时间点,处死动物,观察样品是否有降解,且进行局部的组织病理观察。
Characterization of the test material 化学测试 according to Table A.1 of EN 13432* determination of Zn, Cu, Ni, Cd, Pb, Hg, Cr, Mo, Se, As, dry content, loss on ignition and total fluorine |
Characterization of the test material 化学测试 according to Table A2 of the DIN CERTCO certification scheme 'Additives harmless to the composting process'* determination of PCB, AOX, PCDD/PCDF |
Characterization of the test material 化学测试 infrared transmission spectroscopy*, per spectrum |
Characterization of the test material 化学测试 cobalt content* |
Characterization of the test material 化学测试 layer thickness* |
Biodegradability tests 生物降解能力测试 according to ISO 14851* determination of aerobic biodegradability in an aqueous medium by measurement of oxygen demand, test temperature: 20 °C, maximum duration: 6 months - basic fee including a test duration of 2months |
Biodegradability tests 生物降解能力测试 according to ISO 14851* determination of aerobic biodegradability in an aqueous medium by measurement of oxygen demand, test temperature: 20 °C, maximum duration: 6 months - test prolongation (after end of 2nd month), per additional month |
Biodegradability tests 生物降解能力测试 according to ISO 14855 / ASTM D 5338* determination of aerobic biodegradability under controlled composting conditions by measurement of the evolved carbon dioxide, test temperature: 10 - 60 °C, maximum duration: 6 months - basic feei ncluding a test duration of 2 months |
Biodegradability tests 生物降解能力测试 according to ISO 14855 / ASTM D 5338* determination of aerobic biodegradability under controlled composting conditions by measurement of the evolved carbon dioxide, test temperature: 10 - 60 °C, maximum duration: 6 months - - test prolongation (after end of 2nd month), per additional month . |
Biodegradability tests 生物降解能力测试 according to ISO 17556 / ASTM D 5988 determination of aerobic biodegradability in natural or artificial soil by measurement of the evolved carbon dioxide, test temperature: 10 - 25 °C basic fee including a test duration of 2 months |
Biodegradability tests 生物降解能力测试 according to ISO 17556 / ASTM D 5988 determination of aerobic biodegradability in natural or artificial soil by measurement of the evolved carbon dioxide, test temperature: 10 - 25 °C test prolongation (after end of 2nd month), per additional month |
Disintegration tests 生物分解 according to EN 14045 / ISO 16929 pilot scale composting test with controlled temperature, moisture and aeration in 2 replications including blanks, determination of quantitative (weight of residual fraction > 2 mm) or qualitative disintegration (referring to residual area), characterization of the obtained compost industrial composting* meets requirements of EN 13432, ASTM D 6400, EN 14995 and of the lab certification scheme 'Products made of compostable materials', duration: 12 weeks + 2 weeks for analyses |
Disintegration tests 生物分解 according to EN 14045 / ISO 16929 pilot scale composting test with controlled temperature, moisture and aeration in 2 replications including blanks, determination of quantitative (weight of residual fraction > 2 mm) or qualitative disintegration (referring to residual area), characterization of the obtained compost industrial composting* home-composting* meets requirements of NF T51-800, AS 5810 and of the lab certification scheme 'Products made of compostable materials for home and garden composting', duration: 26 weeks + 2 weeks for analyses |
Disintegration tests 生物分解 in-house method pilot scale composting test according to the minimum requirements of EN 13432, determination of residual fraction > 2 mm, characterization of the obtained compost, duration: 12 weeks + 2 weeks for analyses |
Disintegration tests 生物分解 Disintegration dynamics As an option for disintegration tests, we offer a documentation of disintegration dynamics by taking subsamples of the tested material in arbitrary intervals, e.g. weekly, for gravimetric and photographic analysis; per sampling |
Ecotoxicity tests 生态无毒测试 with two terrestrial plant species according to OECD guideline 208* modified according to section 8 and appendix E of EN 13432 in combination with a preceding disintegration test according to one of the options under item 3 |
Ecotoxicity tests 生态无毒测试 with two terrestrial plant species according to OECD guideline 208* modified according to section 8 and appendix E of EN 13432 without preceding disintegration test (compost production required). |
Ecotoxicity tests 生态无毒测试 with two terrestrial plant species according to OECD guideline 208* modified according to section 8 and appendix E of EN 13432 after and including a shortened composting process according to the DIN CERTCO certification scheme 'Additives harmless to the composting process' |
Ecotoxicity tests 生态无毒测试 with one lumbricide species according to ASTM E 1676* and the requirements of AS 5810 und EN 13432 in combination with a preceding disintegration test according to one of the options under item 3 . |
Ecotoxicity tests 生态无毒测试 with one lumbricide species according to ASTM E 1676* and the requirements of AS 5810 und EN 13432 without preceding disintegration test (compost production required). |
Ecotoxicity tests 生态无毒测试 with one lumbricide species according to ASTM E 1676* and the requirements of AS 5810 und EN 13432 after and including a shortened composting process according to the DIN CERTCO certification scheme 'Additives harmless to the composting process'. |
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